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Synthesis and structure of dinitrato Di(N-dodecanoylpyrrolidine) uranyl(II) | |
Han, JT(韩景田); Bao, BR(包伯荣); Sun, GX(孙国新); Yang, Y; Yang, YH; Chen, MQ; Sun, SX | |
2000 | |
Source Publication | ACTA CHIMICA SINICA
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ISSN | 0567-7351 |
Volume | 58Issue:10Pages:1286 |
Abstract | The complex UO2(DOPOD)(2)(NO3)(2) has been prepared and characterized by elemental analysis and IR spectroscopy. The crystal structure of the complex has been determined by four - circle X - ray diffractometer. The complex crystal belongs to the orthorhombic system and space group Pbca, with cell parameters: a=0.9301(5), b=1.7017(2), c=5.1171(11)nm, V=8.099(5)nm(3), Z = 8, D-c = 1.478g/ cm(3),mu>(*) over bar * (MoK alpha) = 4.061mm(-1), F(000) = 3632, final R = 0.0655 and R-w = 0.1907 for 3006 observed reflections [I > 2 sigma>(*) over bar * (I)], The results indicate that uranyl ion is coordinated to six oxygen atoms, four of them are from two nitrate groups and other two are from carbonyl groups of organic ligands. The uranium atom in the structure is hexagonal bipyramid cooperated. |
Indexed By | SCI |
Language | 英语 |
Funding Project | 应物所项目组 |
WOS ID | WOS:000165207800021 |
Citation statistics | |
Document Type | 期刊论文 |
Identifier | http://ir.sinap.ac.cn/handle/331007/10208 |
Collection | 中科院上海原子核所2003年前 |
Recommended Citation GB/T 7714 | Han, JT,Bao, BR,Sun, GX,et al. Synthesis and structure of dinitrato Di(N-dodecanoylpyrrolidine) uranyl(II)[J]. ACTA CHIMICA SINICA,2000,58(10):1286. |
APA | Han, JT.,Bao, BR.,Sun, GX.,Yang, Y.,Yang, YH.,...&Sun, SX.(2000).Synthesis and structure of dinitrato Di(N-dodecanoylpyrrolidine) uranyl(II).ACTA CHIMICA SINICA,58(10),1286. |
MLA | Han, JT,et al."Synthesis and structure of dinitrato Di(N-dodecanoylpyrrolidine) uranyl(II)".ACTA CHIMICA SINICA 58.10(2000):1286. |
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