CAS OpenIR  > 中科院上海原子核所2003年前
[~(14)C-羧基]-1-氨基环丙烷-1-羧酸的合成
李侣; 林奋智
1992-01-31
Source Publication核技术
Issue01
Abstract本文报道以Ba~(14)CO_3为起始原料制备~(14)KCN;合成~(14)C-甘氨酸的对-溴苯甲亚胺衍生物;然后在DMF和无水K_2CO_3体系中;加1、2-二溴乙烷进行环丙烷化;经盐酸水解;得到[~(14)C-羧基]-1-氨基环丙烷-1-羧酸(~(14)C-ACC)。放化产率:K~(14)CN94.3%.~(14)C-甘氨酸90%;~(14)C-ACC52%。化学纯度和放化纯度均达99%。
Indexed ByCNKI
Language中文
Funding Project原子核所项目组
Document Type期刊论文
Identifierhttp://ir.sinap.ac.cn/handle/331007/10668
Collection中科院上海原子核所2003年前
Recommended Citation
GB/T 7714
李侣,林奋智. [~(14)C-羧基]-1-氨基环丙烷-1-羧酸的合成[J]. 核技术,1992(01).
APA 李侣,&林奋智.(1992).[~(14)C-羧基]-1-氨基环丙烷-1-羧酸的合成.核技术(01).
MLA 李侣,et al."[~(14)C-羧基]-1-氨基环丙烷-1-羧酸的合成".核技术 .01(1992).
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