CAS OpenIR  > 中科院上海原子核所2003年前
~(14)C-~3H双标记炔诺酮庚酸酯的合成
赵夏令; 张雨龙; 何蔚瑜; 张星岳
1981-03-02
Source Publication核技术
Issue02
Abstract<正> 炔诺酮庚酸酯是一种长效避孕药。为了研究该药在体内的吸收分布、代谢过程和作用机制;我们合成了~(14)C-~3H双标记炔诺酮庚酸酯。首先制备了炔诺酮-6;7-~3H和庚酸钠-1-~(14)C。前者系用19-去甲基-Δ~(4.6)-雄烯-3;17-二酮为原料;通过钯-碳酸钙催化氚化;用炔锂乙二胺络合物炔化制得。后者用格氏反应制得。然后两者分别进一步酯化成炔诺酮-6;7-~3H庚酸酯与炔诺酮庚酸酯-1′-~(14)C;并按一定比例相互混合成双标记分子。
Indexed ByCNKI
Language中文
Funding Project原子核所项目组
Document Type期刊论文
Identifierhttp://ir.sinap.ac.cn/handle/331007/10693
Collection中科院上海原子核所2003年前
Recommended Citation
GB/T 7714
赵夏令,张雨龙,何蔚瑜,等. ~(14)C-~3H双标记炔诺酮庚酸酯的合成[J]. 核技术,1981(02).
APA 赵夏令,张雨龙,何蔚瑜,&张星岳.(1981).~(14)C-~3H双标记炔诺酮庚酸酯的合成.核技术(02).
MLA 赵夏令,et al."~(14)C-~3H双标记炔诺酮庚酸酯的合成".核技术 .02(1981).
Files in This Item: Download All
File Name/Size DocType Version Access License
~(14)C-~3H双标记炔诺酮庚酸酯的(464KB) 开放获取LicenseView Download
Related Services
Recommend this item
Bookmark
Usage statistics
Export to Endnote
Google Scholar
Similar articles in Google Scholar
[赵夏令]'s Articles
[张雨龙]'s Articles
[何蔚瑜]'s Articles
Baidu academic
Similar articles in Baidu academic
[赵夏令]'s Articles
[张雨龙]'s Articles
[何蔚瑜]'s Articles
Bing Scholar
Similar articles in Bing Scholar
[赵夏令]'s Articles
[张雨龙]'s Articles
[何蔚瑜]'s Articles
Terms of Use
No data!
Social Bookmark/Share
File name: ~(14)C-~3H双标记炔诺酮庚酸酯的合成.pdf
Format: Adobe PDF
All comments (0)
No comment.
 

Items in the repository are protected by copyright, with all rights reserved, unless otherwise indicated.