CAS OpenIR  > 中科院上海原子核所2003年前
氚(氘)标记秋水仙碱的合成
林奋智; 叶元龙
1984-03-01
Source Publication核技术
Issue02
Abstract本工作介绍了秋水仙碱用0.2N HCl水解成秋水仙裂碱;然后以二氧六环为溶剂使秋水仙裂碱和氚(氘)水进行同位素交换;再用重氮甲烷的乙醚溶液甲基化。经过硅胶纸上行层析法分离纯化获得产品。经红外、紫外、质谱、硅胶纸层析鉴定;确定所得到的产品为秋水仙碱。氘标记物的氘化率为23%;氚标记物放射性比度为4.74Ci/mmol;放化纯度大子98%。
Indexed ByCNKI
Language中文
Funding Project原子核所项目组
Document Type期刊论文
Identifierhttp://ir.sinap.ac.cn/handle/331007/11166
Collection中科院上海原子核所2003年前
Recommended Citation
GB/T 7714
林奋智,叶元龙. 氚(氘)标记秋水仙碱的合成[J]. 核技术,1984(02).
APA 林奋智,&叶元龙.(1984).氚(氘)标记秋水仙碱的合成.核技术(02).
MLA 林奋智,et al."氚(氘)标记秋水仙碱的合成".核技术 .02(1984).
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