CAS OpenIR  > 中科院上海原子核所2003年前
辛酸─1—~(13)C的合成与分析
王惠琼; 赵夏令; 唐国忠
2000
Source Publication核技术
Issue02
Abstract将以溴代正庚烷为原料合成的格氏试剂溴化正庚基镁与Ba13CO3和浓H2SO4作用产生的13CO2进行羧化反应;通过水解;提纯;制得辛酸─1─13C;产率可达90%─93%。用薄层层析对其进行了定性分析;利用MS、IR、1H-NMR和13C-NMR对其进行了结构分析和测定13C丰度(89.5%);并按口服药物的质量要求;用ICP-AES和AFS方法对有关金属元素进行了定量测定。
Indexed ByCNKI
Language中文
Funding Project原子核所项目组
Document Type期刊论文
Identifierhttp://ir.sinap.ac.cn/handle/331007/12156
Collection中科院上海原子核所2003年前
Recommended Citation
GB/T 7714
王惠琼,赵夏令,唐国忠. 辛酸─1—~(13)C的合成与分析[J]. 核技术,2000(02).
APA 王惠琼,赵夏令,&唐国忠.(2000).辛酸─1—~(13)C的合成与分析.核技术(02).
MLA 王惠琼,et al."辛酸─1—~(13)C的合成与分析".核技术 .02(2000).
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