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Preparation of ultrafine-grain graphite by liquid dispersion technique for inhibiting the liquid fluoride salt infiltration | |
Lian, PF; Song, JL; Liu, ZJ; Zhang, JP; Zhao, YL; Gao, YT; Tao, ZC; He, ZT; Gao, LN; Xia, HH; Guo, QG; Huai, P; Zhou, XT; Liu, ZJ (reprint author), Chinese Acad Sci, Inst Coal Chem, Key Lab Carbon Mat, Taiyuan 030001, Peoples R China.; Huai, P (reprint author), Chinese Acad Sci, Shanghai Inst Appl Phys, Key Lab Nucl Radiat & Nucl Energy Technol, Shanghai 201800, Peoples R China. | |
2016 | |
Source Publication | CARBON
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ISSN | 0008-6223 |
Volume | 102Issue:-Pages:208—215 |
Subtype | 期刊文献 |
Abstract | In this work, the mixtures of coke aggregates and coal tar pitch were used as starting materials to prepare ultrafine-grain graphites (UGG) by a liquid mixing method for the inhibition of molten salts in molten salt reactor (MSR). The average diameters of coke aggregates for UGG-1 and UGG-2 were respectively 10 and 5 mu m. The liquid dispersion technique could effectively prevent fine particles of raw materials from being conglomerated. Microstructure, thermophysical and other properties of the obtained graphite were studied. A high-pressure reactor was constructed to evaluate the molten salt penetration in the graphite. Compared to isostatic graphite (IG-110, TOYO TANSO CO., LTD.), UGG-2 possessed excellent properties such as high bending strength of 81.0 +/- 2.5 MPa, compressive strength of 133 +/- 3 MPa, low porosity of 14.0 +/- 0.1% and an average pore diameter of 0.52 +/- 0.01 mm. The fluoride salt volume occupation of IG-110 and UGG-1 under 1.5 atm was 14.4% and 3.7%, respectively. While the volume occupations of UGG-2 under 1.5 atm was only 0.17%, and continued to be steady even up to 5 atm with the increase of 0.45%, less than the critical index proposed for MSR of 0.5%. The UGG-2 could effectively inhibit liquid fluoride salt infiltration and was a promising candidate as neutron moderator or reflector materials for MSR. (C) 2016 Elsevier Ltd. All rights reserved. |
Keyword | Pressure Infiltration Nuclear Graphite Conductivity Foams |
DOI | 10.1016/j.carbon.2016.02.018 |
Indexed By | SCI |
Language | 英语 |
WOS ID | WOS:000372808200023 |
Citation statistics | |
Document Type | 期刊论文 |
Identifier | http://ir.sinap.ac.cn/handle/331007/25810 |
Collection | 中科院上海应用物理研究所2011-2020年 |
Corresponding Author | Song, JL; Liu, ZJ (reprint author), Chinese Acad Sci, Inst Coal Chem, Key Lab Carbon Mat, Taiyuan 030001, Peoples R China.; Huai, P (reprint author), Chinese Acad Sci, Shanghai Inst Appl Phys, Key Lab Nucl Radiat & Nucl Energy Technol, Shanghai 201800, Peoples R China. |
Recommended Citation GB/T 7714 | Lian, PF,Song, JL,Liu, ZJ,et al. Preparation of ultrafine-grain graphite by liquid dispersion technique for inhibiting the liquid fluoride salt infiltration[J]. CARBON,2016,102(-):208—215. |
APA | Lian, PF.,Song, JL.,Liu, ZJ.,Zhang, JP.,Zhao, YL.,...&Huai, P .(2016).Preparation of ultrafine-grain graphite by liquid dispersion technique for inhibiting the liquid fluoride salt infiltration.CARBON,102(-),208—215. |
MLA | Lian, PF,et al."Preparation of ultrafine-grain graphite by liquid dispersion technique for inhibiting the liquid fluoride salt infiltration".CARBON 102.-(2016):208—215. |
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