The development of TXRF method and its application on the study of trace elements in water at SSRF
Wang, LL; Yu, HS; Li, LN; Wei, XJ; Huang, YY; Huang, YY (reprint author), Chinese Acad Sci, Shanghai Inst Appl Phys, Shanghai Synchrotron Radiat Facil, Zhangheng Rd 239, Shanghai 201204, Peoples R China.
2016
发表期刊NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION B-BEAM INTERACTIONS WITH MATERIALS AND ATOMS
ISSN0168-583X
卷号375期号:-页码:49—55
文章类型期刊文献
摘要The objective of this study is the development of Total Reflection X-ray Fluorescence (TXRF) method at Shanghai Synchrotron Radiation Facility (SSRF). In this paper, the SR-TXRF setup and the related experimental methods and results for the determination of trace elements in water were described. Compared with the conventional lab TXRF, the detection limits obtained in our experiment are very lower due to the advantages of synchrotron radiation, which varied from 1.11 pg (Cr) to 0.28 pg (Zn). The average deviation of the specimen replicates is below 5%, and the deviations of measured element concentrations for Cr, Mn, Co, Ni and Cu by SR-TXRF are within 10% compared with the values by ICP-MS, so our TXRF results are agreed with those obtained by ICP-MS for the detected metals. Based on the results, the SR-TXRF setup and method have been feasible for the quantitative analysis of multi-elements in water at SSRF and that will play an important role in the research area for the environmental liquid samples analysis. (C) 2016 Elsevier B.V. All rights reserved.
关键词X-ray-fluorescence Total-reflection Synchrotron-radiation Sr-txrf Spectrometry Samples Brazil Films
DOI10.1016/j.nimb.2016.03.046
收录类别SCI
语种英语
WOS记录号WOS:000375808400009
引用统计
被引频次:3[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.sinap.ac.cn/handle/331007/25861
专题中科院上海应用物理研究所2011-2018年
通讯作者Huang, YY (reprint author), Chinese Acad Sci, Shanghai Inst Appl Phys, Shanghai Synchrotron Radiat Facil, Zhangheng Rd 239, Shanghai 201204, Peoples R China.
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Wang, LL,Yu, HS,Li, LN,et al. The development of TXRF method and its application on the study of trace elements in water at SSRF[J]. NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION B-BEAM INTERACTIONS WITH MATERIALS AND ATOMS,2016,375(-):49—55.
APA Wang, LL,Yu, HS,Li, LN,Wei, XJ,Huang, YY,&Huang, YY .(2016).The development of TXRF method and its application on the study of trace elements in water at SSRF.NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION B-BEAM INTERACTIONS WITH MATERIALS AND ATOMS,375(-),49—55.
MLA Wang, LL,et al."The development of TXRF method and its application on the study of trace elements in water at SSRF".NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION B-BEAM INTERACTIONS WITH MATERIALS AND ATOMS 375.-(2016):49—55.
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