In situ synchrotron small- and wide-angle X-ray study on the structural evolution of Kevlar fiber under uniaxial stretching
Li, XY; Tian, F; Zhou, P; Yang, CM; Li, XH; Bian, FG; Wang, J; Li, XH (reprint author), Chinese Acad Sci, Shanghai Inst Appl Phys, Shanghai Synchrotron Radiat Facil, Shanghai, Peoples R China.
2016
发表期刊RSC ADVANCES
ISSN2046-2069
卷号6期号:85页码:81552-81558
文章类型期刊论文
摘要The structural evolution and mechanism of Kevlar 29 and Kevlar 129 (poly(p-phenylene terephthalamide)) fibers during stretching were studied by in situ synchrotron small-angle X-ray scattering (SAXS) and wide-angle X-ray scattering (WAXS). Compared with Kevlar 29, the tensile strength of Kevlar 129 increased, while the elongation-to-break ratio decreased. SAXS results showed that ordered lamellae were observed only in Kevlar 29. The fibril length of Kevlar 129 was larger than that of Kevlar 29; however, the fibril misorientation width of Kevlar 129 was smaller. During stretching, both the fibril length and fibril misorientation width decreased at low strains, and then increased until the fibrils broke both in Kevlar 29 and Kevlar 129 fibers. From WAXS results, the crystal orientation angle decreased in Kevlar 29 during stretching, while that in Kevlar 129 increased at low strains and then decreased until the fibers broke. The change of crystallinity indicated that the amorphous phase can convert to the crystal phase at high strains, although the conversion ratio was not large. By combining the SAXS and WAXS results, a potential mechanism for Kevlar fibers during stretching was proposed.
DOI10.1039/c6ra17671b
收录类别SCI
语种英语
WOS记录号WOS:000382776000013
引用统计
被引频次:3[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.sinap.ac.cn/handle/331007/26538
专题中科院上海应用物理研究所2011-2018年
通讯作者Yang, CM; Li, XH (reprint author), Chinese Acad Sci, Shanghai Inst Appl Phys, Shanghai Synchrotron Radiat Facil, Shanghai, Peoples R China.
推荐引用方式
GB/T 7714
Li, XY,Tian, F,Zhou, P,et al. In situ synchrotron small- and wide-angle X-ray study on the structural evolution of Kevlar fiber under uniaxial stretching[J]. RSC ADVANCES,2016,6(85):81552-81558.
APA Li, XY.,Tian, F.,Zhou, P.,Yang, CM.,Li, XH.,...&Li, XH .(2016).In situ synchrotron small- and wide-angle X-ray study on the structural evolution of Kevlar fiber under uniaxial stretching.RSC ADVANCES,6(85),81552-81558.
MLA Li, XY,et al."In situ synchrotron small- and wide-angle X-ray study on the structural evolution of Kevlar fiber under uniaxial stretching".RSC ADVANCES 6.85(2016):81552-81558.
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