Reconstruction of the Wet Chemical Synthesis Process: The Case of Fe5C2 Nanoparticles
Yao, SY; Yang, C; Zhao, HB; Li, SW; Lin, LL; Wen, W; Liu, JX; Hu, G; Li, WX; Hou, YL; Ma, D
2017
发表期刊JOURNAL OF PHYSICAL CHEMISTRY C
ISSN1932-7447
卷号121期号:9页码:5154-5160
文章类型期刊论文
摘要Wet chemical synthesis (WCS), especially under high temperatures, is one of the most frequently used strategies for nanostructured material construction, which has been used extensively in medical-, energy-, and environment-related applications. Although knowledge about the WCS process has been accumulated in the past two decades, the high temperature used in the process and multiphase nature of intermediates and products are key factors preventing the processes from rationalization. In this paper, by using multilevel in situ cells, we developed a strategy to monitor the reaction details of WCS processed in the solid, liquid, and gas phase simultaneously. This protocol has proven successful to reconstruct the WCS process of Fe5C2 nanoparticles (NPs) and unravel the complicated chemistry in the synthesis process.
DOI10.1021/acs.jpcc.7b00198
收录类别SCI
语种英语
WOS记录号WOS:000396295800041
引用统计
文献类型期刊论文
条目标识符http://ir.sinap.ac.cn/handle/331007/27433
专题中科院上海应用物理研究所2011-2018年
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GB/T 7714
Yao, SY,Yang, C,Zhao, HB,et al. Reconstruction of the Wet Chemical Synthesis Process: The Case of Fe5C2 Nanoparticles[J]. JOURNAL OF PHYSICAL CHEMISTRY C,2017,121(9):5154-5160.
APA Yao, SY.,Yang, C.,Zhao, HB.,Li, SW.,Lin, LL.,...&Ma, D.(2017).Reconstruction of the Wet Chemical Synthesis Process: The Case of Fe5C2 Nanoparticles.JOURNAL OF PHYSICAL CHEMISTRY C,121(9),5154-5160.
MLA Yao, SY,et al."Reconstruction of the Wet Chemical Synthesis Process: The Case of Fe5C2 Nanoparticles".JOURNAL OF PHYSICAL CHEMISTRY C 121.9(2017):5154-5160.
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