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The effect of ball-milling time and annealing temperature on fracture toughness of Ni-3 wt.% SiC using small punch testing
Yang, C; Wei, T; Muransky, O; Carr, D; Huang, HF; Zhou, XT
2018
Source PublicationMATERIALS CHARACTERIZATION
ISSN1044-5803
Volume138Pages:289-295
Subtype期刊论文
AbstractA set of dispersion strengthened Ni-3 wt.% SiC samples have been prepared via a powder metallurgy route for an application in molten salt reactor (MSR) systems. A mixture of 97 wt.% Ni and 3 wt.% SiC powder was prepared by varying the ball-milling time (8, 24, 36 and 48 h). The ball-milling process was followed by powder consolidation using spark plasma sintering (SPS) and rapid cooling to room temperature. The samples were then annealed at different temperatures (300 degrees C, 700 degrees C and 850 degrees C). The fracture behaviour of the Ni-3 wt.% SiC samples was investigated using the Small Punch Test (SPT). A scanning electron microscope (SEM) with energy dispersive spectrometer (EDS) and electron back-scatter diffraction (EBSD), as well as transmission electron microscopy (TEM) were employed to examine the microstructure of the tested Ni-3 wt.% SiC samples. The obtained results show that the SPT fracture energy is strongly dependent on the grain size of Ni matrix, which is affected by ball-milling times and annealing temperature. It has been further found that the segregation of large SiC particles at grain boundaries promotes intergranular fracture and thus significantly reduces the fracture energy. The results indicate that the distribution and size of SiC particles at grain boundary is mainly affected by the ball-milling time. Hence, the ball-milling time governs the fracture toughness of Ni-3 wt.% SiC samples.
KeywordMetal-matrix Composites Ion irradiatIon Alloy Nanoparticles Embrittlement Dispersion Reactor Steels Damage
DOI10.1016/j.matchar.2018.02.024
Indexed BySCI
Language英语
WOS IDWOS:000428483400032
Citation statistics
Document Type期刊论文
Identifierhttp://ir.sinap.ac.cn/handle/331007/29174
Collection中科院上海应用物理研究所2011-2018年
Affiliation1.Yang, C
2.Wei, T
3.Muransky, O
4.Carr, D
5.Huang, HF
6.Zhou, XT
Recommended Citation
GB/T 7714
Yang, C,Wei, T,Muransky, O,et al. The effect of ball-milling time and annealing temperature on fracture toughness of Ni-3 wt.% SiC using small punch testing[J]. MATERIALS CHARACTERIZATION,2018,138:289-295.
APA Yang, C,Wei, T,Muransky, O,Carr, D,Huang, HF,&Zhou, XT.(2018).The effect of ball-milling time and annealing temperature on fracture toughness of Ni-3 wt.% SiC using small punch testing.MATERIALS CHARACTERIZATION,138,289-295.
MLA Yang, C,et al."The effect of ball-milling time and annealing temperature on fracture toughness of Ni-3 wt.% SiC using small punch testing".MATERIALS CHARACTERIZATION 138(2018):289-295.
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