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| Radiolabeling of 1-[N ',N '-bis(2-chloroethyl)-4-aminophenyl]-N-methyl-fullereno-C-60-[1,9-c]pyrrolidine with I-125 | |
| Ran, TC（冉铁成）; Liu, RL（刘瑞丽）; Yin, JJ（尹娟娟）; Zhu, JH; Li, WX（李文新）; Li, QN（李晴暖）; Ran, TC (reprint author), Chinese Acad Sci, Shanghai Inst Appl Phys, Shanghai 201800, Peoples R China | |
| 2006 | |
| Source Publication | JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY
 |
| ISSN | 0236-5731 |
| Volume | 268Issue:3Pages:599 |
| Abstract | A procedure for labeling of a fullerene derivative 1-[N',N'-bis(2-chloroethyl)-4-aminophenyl]-N-methyl-fullereno-C-50-[1.9-c]pyrrolidine (C-60-C13H18N2Cl2) with I-125 is reported. The compound was first iodinated with a large excess of iodine monochloride and then radiolabeled by isotopic exchange with (NaI)-I-125 in a toluene-water two-phase system. The dependence of the radiolabeling yield on the reaction temperature and exchange time was examined. The radiolabeling yield of the compound was as high as 94% after heating for 2 hours at 130 degrees C. |
| Subject Area | Chemistry |
| Indexed By | SCI |
| Language | 英语 |
| Funding Project | 应物所项目组 |
| WOS ID | WOS:000238843600022 |
| Citation statistics | |
| Document Type | 期刊论文 |
| Identifier | http://ir.sinap.ac.cn/handle/331007/8177 |
| Collection | 中科院上海应用物理研究所2004-2010年 |
| Corresponding Author | Ran, TC (reprint author), Chinese Acad Sci, Shanghai Inst Appl Phys, Shanghai 201800, Peoples R China |
| Recommended Citation GB/T 7714 | Ran, TC,Liu, RL,Yin, JJ,et al. Radiolabeling of 1-[N ',N '-bis(2-chloroethyl)-4-aminophenyl]-N-methyl-fullereno-C-60-[1,9-c]pyrrolidine with I-125[J]. JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY,2006,268(3):599. |
| APA | Ran, TC.,Liu, RL.,Yin, JJ.,Zhu, JH.,Li, WX.,...&Ran, TC .(2006).Radiolabeling of 1-[N ',N '-bis(2-chloroethyl)-4-aminophenyl]-N-methyl-fullereno-C-60-[1,9-c]pyrrolidine with I-125.JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY,268(3),599. |
| MLA | Ran, TC,et al."Radiolabeling of 1-[N ',N '-bis(2-chloroethyl)-4-aminophenyl]-N-methyl-fullereno-C-60-[1,9-c]pyrrolidine with I-125".JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY 268.3(2006):599. |
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