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Radiolabeling of 1-[N ',N '-bis(2-chloroethyl)-4-aminophenyl]-N-methyl-fullereno-C-60-[1,9-c]pyrrolidine with I-125
Ran, TC(冉铁成); Liu, RL(刘瑞丽); Yin, JJ(尹娟娟); Zhu, JH; Li, WX(李文新); Li, QN(李晴暖); Ran, TC (reprint author), Chinese Acad Sci, Shanghai Inst Appl Phys, Shanghai 201800, Peoples R China
2006
Source PublicationJOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY
ISSN0236-5731
Volume268Issue:3Pages:599
AbstractA procedure for labeling of a fullerene derivative 1-[N',N'-bis(2-chloroethyl)-4-aminophenyl]-N-methyl-fullereno-C-50-[1.9-c]pyrrolidine (C-60-C13H18N2Cl2) with I-125 is reported. The compound was first iodinated with a large excess of iodine monochloride and then radiolabeled by isotopic exchange with (NaI)-I-125 in a toluene-water two-phase system. The dependence of the radiolabeling yield on the reaction temperature and exchange time was examined. The radiolabeling yield of the compound was as high as 94% after heating for 2 hours at 130 degrees C.
Subject AreaChemistry
Indexed BySCI
Language英语
Funding Project应物所项目组
WOS IDWOS:000238843600022
Citation statistics
Cited Times:3[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.sinap.ac.cn/handle/331007/8177
Collection中科院上海应用物理研究所2004-2010年
Corresponding AuthorRan, TC (reprint author), Chinese Acad Sci, Shanghai Inst Appl Phys, Shanghai 201800, Peoples R China
Recommended Citation
GB/T 7714
Ran, TC,Liu, RL,Yin, JJ,et al. Radiolabeling of 1-[N ',N '-bis(2-chloroethyl)-4-aminophenyl]-N-methyl-fullereno-C-60-[1,9-c]pyrrolidine with I-125[J]. JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY,2006,268(3):599.
APA Ran, TC.,Liu, RL.,Yin, JJ.,Zhu, JH.,Li, WX.,...&Ran, TC .(2006).Radiolabeling of 1-[N ',N '-bis(2-chloroethyl)-4-aminophenyl]-N-methyl-fullereno-C-60-[1,9-c]pyrrolidine with I-125.JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY,268(3),599.
MLA Ran, TC,et al."Radiolabeling of 1-[N ',N '-bis(2-chloroethyl)-4-aminophenyl]-N-methyl-fullereno-C-60-[1,9-c]pyrrolidine with I-125".JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY 268.3(2006):599.
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