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二硝酸 N ,N '-二癸酰基哌嗪合铀酰髤配合物的合成和晶体结构
包伯荣; 韩阳; 曹卫国; 杨兴存; 陈民勤
Source Publication无机化学学报
Other AbstractThe complex UO2(DDPEZ)(NO3)2 has been prepared and characterized by IR spectroscopy and XPS spectra. The crystal structure of the complex has been determined by X-ray diffraction. The crystal belongs to Triclinic system and space group P1, with cell parameters: a=0.664 2(3) nm, b=0.805 0(2) nm, c=1.515 6(5) nm, α=104.39(2)°, β=91.13(3)°, γ=94.84(3)°, and V=0.781 4(5) nm3, Z=2, Dc=1 676 kg·m-3, μ(Mo Kα)=0.071 073 nm, F(000)=390, final R=0.037 9 and wR=0.091 7 for observed reflections[I>2σ(I)]. The results indicated that uranyl ion is coordinated with six oxygen atoms, four of them from two nitrate groups and two from carbonyl groups of different organic ligands. CCDC: 284452.
Keywordn N'-二癸酰基哌嗪 晶体结构 合成 铀酰髤配合物
Indexed ByCNKI
Funding Project应物所项目组
Document Type期刊论文
Corresponding Author包伯荣
Recommended Citation
GB/T 7714
包伯荣,韩阳,曹卫国,等. 二硝酸 N ,N '-二癸酰基哌嗪合铀酰髤配合物的合成和晶体结构[J]. 无机化学学报,2006(2).
APA 包伯荣,韩阳,曹卫国,杨兴存,&陈民勤.(2006).二硝酸 N ,N '-二癸酰基哌嗪合铀酰髤配合物的合成和晶体结构.无机化学学报(2).
MLA 包伯荣,et al."二硝酸 N ,N '-二癸酰基哌嗪合铀酰髤配合物的合成和晶体结构".无机化学学报 .2(2006).
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