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SOLID-STATE REACTION BETWEEN P-BENZOQUINONE AND 4,4 '-BIPHENOL: A THz TIME-DOMAIN SPECTROSCOPIC STUDY
Liu, Guifeng(刘桂锋); Zhao, Hongwei(赵红卫); Liu, Xiaohong; Wang, Wenfeng(王文锋)
2011
Source PublicationJOURNAL OF APPLIED SPECTROSCOPY
ISSN0021-9037
Volume78Issue:3Pages:318
AbstractTerahertz time-domain spectroscopy (THz-TDS) was employed to record the progress of the reaction between p-benzoquinone (BQ) and 4,4'-biphenol (4BP) in the solid state. Through the THz-TDS, distinct absorption peaks of reactants and products were obtained. Sample preparations in the solid state, with and without grinding, influenced the conversion kinetics. Several kinetic equations or models were tried to fit the reaction data. A kinetic rate constant was obtained, with the reaction observed to be consistent with diffusion-controlled mechanisms. Differential scanning calorimetry and X-ray powder diffraction analyses were also used to characterize the solid-state reaction and products. The study shows that THz spectroscopy is a promising tool in evaluating the complex formation through solid-state reactions.
Indexed BySCI
Language英语
Funding Project应物所项目组
WOS IDWOS:000294010700003
Citation statistics
Document Type期刊论文
Identifierhttp://ir.sinap.ac.cn/handle/331007/9590
Collection中科院上海应用物理研究所2011-2019年
Recommended Citation
GB/T 7714
Liu, Guifeng,Zhao, Hongwei,Liu, Xiaohong,et al. SOLID-STATE REACTION BETWEEN P-BENZOQUINONE AND 4,4 '-BIPHENOL: A THz TIME-DOMAIN SPECTROSCOPIC STUDY[J]. JOURNAL OF APPLIED SPECTROSCOPY,2011,78(3):318.
APA Liu, Guifeng,Zhao, Hongwei,Liu, Xiaohong,&Wang, Wenfeng.(2011).SOLID-STATE REACTION BETWEEN P-BENZOQUINONE AND 4,4 '-BIPHENOL: A THz TIME-DOMAIN SPECTROSCOPIC STUDY.JOURNAL OF APPLIED SPECTROSCOPY,78(3),318.
MLA Liu, Guifeng,et al."SOLID-STATE REACTION BETWEEN P-BENZOQUINONE AND 4,4 '-BIPHENOL: A THz TIME-DOMAIN SPECTROSCOPIC STUDY".JOURNAL OF APPLIED SPECTROSCOPY 78.3(2011):318.
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